4.3 Article

Hydrothermal synthesis of fine MoS2 crystals from Na2MoO4 and KSCN

Journal

CHEMISTRY LETTERS
Volume 32, Issue 8, Pages 768-769

Publisher

CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2003.768

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A fine crystal MoS2 has been synthesized by hydrothermal method in a clean and efficient system consisting of Na2MoO4 and KSCN in a short time (24h). The product is characterized by XRD and TEM, and the ED pattern reveals a hexagonal crystal. The mechanism of this reaction is also put forward. Thus this method provides us a new routine to synthesize other transition metal sulfides.

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