Journal
ORGANIC LETTERS
Volume 5, Issue 16, Pages 2959-2962Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0351192
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A total solid-phase synthesis of lamellarins U and L has been achieved. The conversion of an aldehyde group into a formate by a Baeyer-Villiger reaction and a intramolecular [3 + 2] cycloaddition of a 3,4-dihydroisoquinolinium salt over a triple bond comprise the key steps of the process. Each transformation has been controlled with the proper spectroscopic and analytical methods.
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