Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 68, Issue 16, Pages 6463-6465Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo034281f
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In one step, the skeleton of cis-spirovetivanes was constructed with high stereoselectivity by the phosphine-catalyzed [3+2] cycloaddition reaction of tert-butyl 2,3-butadienoate or 2-butynoate with 3-methyl-2-methylenecyclohexanone (5). This method was exemplified by the first highly efficient total synthesis of natural product (-)-hinesol, which is an active ingredient of cerebral circulation and metabolism improvers.
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