Journal
JOURNAL OF APPLIED POLYMER SCIENCE
Volume 89, Issue 8, Pages 2036-2040Publisher
WILEY
DOI: 10.1002/app.12346
Keywords
annealing; differential scanning calorimetry (DSC); nanocomposites; polymorphism; WAXS
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Polymorphism in poly(vinylidene fluoride) (PVDF)/clay nanocomposites was studied. Poly(vinylidene fluoride)/clay nanocomposites were prepared with melt intercalation. The samples were characterized with X-ray diffraction, differential scanning calorimetry, and Fourier transform infrared spectroscopy. The nanocomposite exhibited the 0 form. Thermal annealing performed at 125 and 185'C showed that the 0 form of PVDF was stable. The stability of the P form of PVDF was ascertained from these studies. The 0 form of PVDF in the nanocomposites could be due to crystallization in the constrained phase. (C) 2003 Wiley Periodicals, Inc.
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