Journal
JOURNAL OF NATURAL PRODUCTS
Volume 66, Issue 9, Pages 1263-1265Publisher
AMER CHEMICAL SOC
DOI: 10.1021/np030115r
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The absolute stereochemistry of the sponge metabolite cyclosmenospongine (1) was determined as 5R, 8S, 9R, 10S by chemical correlation. Substitution of the methoxyl group by an amino group in the cyclic product 3 of acid-catalyzed rearrangement of ilimaquinone (5) afforded cyclosmenospongine 1. Cyclosmenospongine was also obtained by acid-catalyzed cyclization of smenospongine (6).
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