Journal
CHEMISTRY OF MATERIALS
Volume 15, Issue 18, Pages 3450-3462Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm034167d
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The reduction of diazonium salts in an aprotic medium permits the attachment of substituted aryl groups to a variety of metals: Co, Ni, Cu, Zn, Pt, and Au. These aryl groups are strongly bonded to the metal as they resist sustained rinsing under sonication in organic solvents. The organic layers have been characterized by cyclic voltammetry, infrared reflection absorption spectroscopy, X-ray photoelectron spectroscopy, Rutherford backscattering, electrochemical impedance spectroscopy, and atomic force microscopy. From these data it is possible to propose a structure for these grafted layers.
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