Journal
MATERIALS CHEMISTRY AND PHYSICS
Volume 82, Issue 1, Pages 206-209Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/S0254-0584(03)00206-2
Keywords
chalcogenides; chemical synthesis; electron microscopy
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Metal sulfides MS (M = Cd, Zn, Co, Pb, CU), M2S3 (M = Bi, Sb), M2S (M = Ag) were successfully synthesized through a one-step reaction between metal salts and thiourea in ethylene glycol (EG) under the microwave irradiation. The products were characterized by powder X-ray diffraction (XRD), X-ray photoelectron spectroscope (XPS), transmission electron microscope (TEM) and electron diffraction (ED). (C) 2003 Elsevier B.V. All rights reserved.
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