Journal
SCRIPTA MATERIALIA
Volume 49, Issue 8, Pages 773-778Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S1359-6462(03)00429-9
Keywords
mechanical milling; Raman spectroscopy; X-ray diffraction; nanocrystalline materials
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Silicon particles with nanometric size were synthesized by mechanical milling using a high-energy ball miller. The Si nanoparticles, observed using Raman spectroscopy, were formed according to a solid-phase reaction between amorphous SiO2 and Al powders. The crystalline size was determined by fitting the Raman spectrum with a phonon confinement model. (C) 2003 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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