Journal
ORGANIC LETTERS
Volume 5, Issue 20, Pages 3667-3669Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol035355c
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Funding
- NIGMS NIH HHS [GM 58160] Funding Source: Medline
- NCPDCID CDC HHS [CI T32CA09112] Funding Source: Medline
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A general and efficient copper-catalyzed method for the amidation of vinyl bromides and iodides has been developed. This protocol uses a combination of 5 mol % copper iodide and 20 mol % N,N'-dimethyl ethylenediamine. Substrates bearing ester, silyl ether, and amino groups were successfully coupled under the reaction conditions. The double bond geometry of the vinyl halides was retained under the reaction conditions.
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