Journal
CHEMISTRY LETTERS
Volume 32, Issue 10, Pages 898-899Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2003.898
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Radical-mediated single carbonylation of alkyl iodides furnishing carboxylic acids proceeded in water using phosphinic acid as a radical initiator in the presence of a surfactant (CTAB). On the other hand, formation of double carbonylation product (alpha-keto carboxylic acid) along with single carbonylation product was observed for the first time, when the reaction was carried out in aqueous ethanol without any surfactants.
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