Journal
TETRAHEDRON LETTERS
Volume 44, Issue 42, Pages 7779-7781Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2003.08.081
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A convenient sequential oxidation-olefination protocol is reported using tetra-n-propylammonium perruthenate (TPAP) as oxidant and phosphonium salts as olefin source. The oxidation reaction mixture is added directly to the phosphorane facilitating an efficient method for this transformation that avoids work-up of potentially sensitive aldehyde intermediates. (C) 2003 Elsevier Ltd. All rights reserved.
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