Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 125, Issue 41, Pages 12527-12530Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja0363258
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Funding
- NIGMS NIH HHS [R01-GM62871] Funding Source: Medline
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A single method (2% Pd-2(dba)(3)/8% PCyp(3)/NMI in THF/NMP at 80 degreesC; Cyp = cyclopentyl) achieves the cross-coupling of a range of beta-hydrogen-containing primary alkyl iodides, bromides, chlorides, and tosylates with an array of alkyl-, alkenyl-, and arylzinc halides. The process is compatible with a variety of functional groups, including esters, amides, imides, nitriles, and heterocycles.
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