Journal
ORGANIC LETTERS
Volume 5, Issue 21, Pages 3955-3957Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol035616i
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Initial studies of a rare exocyclic C-O bond carbonylation are reported. Under the catalysis of Co-2(CO)(8) in the absence of HI as the copromoter, cycloimino esters are carbonylated to afford N-acyllactams in high yields under relatively mild conditions (100-160 degreesC and 200-1000 psi). The reaction is interesting because it opens up the possibility of carbonylation of alcohols in the absence of HI.
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