Journal
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume 51, Issue 26, Pages 7547-7554Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jf0346354
Keywords
acrylamide; exploratory; FDA; food survey; liquid chromatography-tandem mass spectrometry; LC-MS/MS; method
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The described liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the detection of acrylamide in food entails aqueous room temperature extraction, SPE cleanup, and analysis by LC-MS/MS. The method is applicable to a wide variety of foods. [C-13(3)]acrylamide is the internal standard. The limit of quantitation is 10 ppb (mug/kg). Data were obtained in duplicate from >450 products representing >35 different food types. The variability in analyte levels in certain food types suggests that it may be possible to reduce acrylamide levels in those foods.
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