Journal
ORGANIC LETTERS
Volume 5, Issue 26, Pages 4987-4990Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol035942y
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[GRAPHICS] A mild intermolecular copper-mediated amination of aryl iodides has been developed. The reaction takes place at room temperature or heating at 90 degreesC and tolerates halogens attached to the aromatic ring. Its synthetic applications include a synthetic protocol for unsymmetrical N,N'-dialkylated phenylenediamines and both a stepwise and a general synthetic method for N-aryl secondary amines via Ns-anilides (readily obtained by reaction of the Ns-amide).
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