Journal
TETRAHEDRON LETTERS
Volume 45, Issue 2, Pages 293-294Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2003.10.189
Keywords
Xyloketal D; total synthesis; ketal formation; marine secondary; metabolites
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(+)-Xyloketal D was prepared in a one-pot multistep domino reaction by heating optically active 5-hydroxy-4-methyl-3-methylenepentan-2-one (R) in toluene with 2,4-dihydroxyacetophenone. The absolute configuration of the natural product was confirmed by preparation of the starting enone from a lactone of established absolute configuration. (C) 2003 Elsevier Ltd. All rights reserved.
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