Journal
JOURNAL OF MOLECULAR STRUCTURE
Volume 688, Issue 1-3, Pages 197-201Publisher
ELSEVIER
DOI: 10.1016/j.molstruc.2003.10.015
Keywords
crystal structure; supramolecular framework; one-dimensional channels; hydrogen bonding; pi-pi stacking interactions
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A new supramolecular compound formulated [Cu(DPC)(H2O)(3)] (H2DPC = Pyridine-2,6-dicarboxylic acid) was synthesized under mild conditions and characterized by elemental analyses, IR spectrum, thermogravimetric (TG) analysis and single-crystal X-ray diffraction. The crystal crystallizes in the monoclinic system, space group of C2/c with a = 6.4448(9) Angstrom, b = 23.192(3) Angstrom, c = 6.9139(12) Angstrom, alpha = 90degrees, beta = 106.622(11)degrees, gamma = 90degrees, V = 990.2(3) Angstrom(3), Z = 4, R = 0.0580, and wR(2) = 0.1522. The compound exhibits an interesting three-dimensional (3D) supramolecular framework structure with one-dimensional channels, which is constructed by extensive hydrogen-bonding and pi-pi stacking interactions. (C) 2003 Elsevier B.V. All rights reserved.
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