Journal
ANALYTICA CHIMICA ACTA
Volume 502, Issue 1, Pages 65-74Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.aca.2003.09.062
Keywords
diuretics; urine; doping; LC-MS-MS; SPE
Categories
Ask authors/readers for more resources
A new method has been developed for the routine detection of diuretics in urine samples collected from athletes. The method developed uses automated solid phase extraction (SPE) with analysis of the extracts by high performance liquid chromatography using electrospray ionisation tandem mass spectrometry. It requires only one injection per sample and is currently capable of detecting 35 diuretics and related compounds at the rate of five samples per hour. All parent compounds can be detected at urinary concentrations significantly below 100 ng/ml with the recovery of most analytes being greater than 80%. Crown Copyright (C) 2003 Published by Elsevier B.V. All rights reserved.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available