Journal
TETRAHEDRON LETTERS
Volume 45, Issue 6, Pages 1183-1185Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2003.11.137
Keywords
Baylis-Hillman reactions; sulpholane; aprotic polar solvent; DABCO; activated olefins
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Sulpholane, a commercially available solvent, is used for the first time as a new solvent for the Baylis-Hillman reaction tinder ambient conditions; a wide variety of olefins as well as aldehydes participate very efficiently resulting in good to excellent yields of products. Acrylamide also underwent the Baylis-Hillman reaction with 4-nitrobenzaldehyde under these reaction conditions. (C) 2003 Elsevier Ltd. All rights reserved.
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