Journal
TETRAHEDRON LETTERS
Volume 45, Issue 7, Pages 1449-1451Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2003.12.037
Keywords
reductive amination; C-2-symmetry; chiral amines; titanium isopropoxide
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A novel one-pot reductive amination of ketones using the combination Ti((OPr)-Pr-i)(4)/H-2/Pd-C is reported. This practical procedure does not require any solvent, and affords C-2-symmetrical secondary amines in high yields and excellent diastereoselectivities. (C) 2003 Elsevier Ltd. All rights reserved.
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