Journal
TETRAHEDRON LETTERS
Volume 45, Issue 10, Pages 2071-2073Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2004.01.071
Keywords
C-60; cucurbit[7]uril; solvent free; high-speed vibration milling; solid-state reaction; [60]fullerene
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The synthesis of a cucurbit[7]uril-[60]fullerene supramolecule complex using a simple, green, and efficent pathway is reported for the first time. In the complex, which was found to be of the 1:2 type, the compounds interact weekly with each other. Since the complexation can be achieved by a solid-solid reaction without solvent both the waste and contact with harmful solvents can by reduced to a minimum. A significant increase of reaction rate and yield compared to the heterogenous complexation was observed. (C) 2004 Published by Elsevier Ltd.
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