Journal
ORGANIC LETTERS
Volume 6, Issue 6, Pages 953-956Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol049979+
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Funding
- NCI NIH HHS [CA-76497] Funding Source: Medline
- NIGMS NIH HHS [GM-65597] Funding Source: Medline
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The title technique is a convenient and powerful method for directly monitoring or assaying any reaction mixture or reagent solution. Examples of some common processes (Fischer esterification, lithiation, butyllithium/THF compatibility, olefin metathesis, and a quantification assay), each interrogated in its native solvent, are presented. The spectral data are easy to acquire, and the information content makes a compelling case for routine use of No-D NMR spectroscopy.
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