Journal
TETRAHEDRON LETTERS
Volume 45, Issue 16, Pages 3241-3243Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2004.02.118
Keywords
Dysidea; polychlorinated amino acids
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The first total synthesis of (2S,4S)-5,5-dichloroleucine has been achieved in 11 steps from L-pyroglutamic acid. A key step is the dichlorination process on the hydrazone of aldehyde 13 with CuCl2 in triethylamine. (C) 2004 Elsevier Ltd. All rights reserved.
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