Journal
ORGANIC LETTERS
Volume 6, Issue 8, Pages 1265-1268Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol049805s
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- NIGMS NIH HHS [GM 50101] Funding Source: Medline
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[GRAPHICS] The radicals formed in Mn(III)-based oxidative free-radical cyclizations of beta-keto esters and malonate esters can be trapped with sodium azide and Mn(ill) to give cyclic and bicyclic azides in 30-80% yield. Reduction of the azide gives bi- and tricyclic lactams.
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