Journal
REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 75, Issue 5, Pages 1251-1254Publisher
AMER INST PHYSICS
DOI: 10.1063/1.1710695
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The design and operation of an electrochemical cell for reflection-mode powder x-ray diffraction experiments are discussed. The cell is designed for the study of electrodes that are used in rechargeable lithium batteries. It is designed for assembly in a glove box so that air-sensitive materials, such as lithium foil electrodes and carbonate-based electrolytes with lithium salts, can be used. The cell uses a beryllium window for x-ray transmission and electrical contact. A simple mechanism for compressing the electrodes is included in the design. Sample results for the cell are shown with a Cu Kalpha source and a position-sensitive detector. (C) 2004 American Institute Of Physics.
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