Journal
JOURNAL OF SOLID STATE CHEMISTRY
Volume 177, Issue 6, Pages 2205-2209Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jssc.2004.01.005
Keywords
one-dimensional nanostructures; MgF2; KMgF3; microemulsion; hydrothermal reactions
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MgF2 nanorods with diameters of 60-100 nm were synthesized by a microemulsion method. Subsequent hydrothermal reaction of as-synthesized MgF2 nanorods and KF at 240degreesC for 3 days or 140degreesC for 7 days resulted in KMgF3 nanorods, which retained the rod-like morphology of the source material MgF2 in the reaction process. The morphology of as-synthesized MgF2 strongly depended on the molar ratio between water and the surfactant CTAB and the concentration of CTAB. (C) 2004 Elsevier Inc. All rights reserved.
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