Journal
MATERIALS RESEARCH BULLETIN
Volume 39, Issue 7-8, Pages 981-986Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2004.03.017
Keywords
inorganic compounds; chalcogenides; chemical synthesis
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MoS2 particles of uniform size (ca. 70 nm) consisting of random and loosely stacked layers have been synthesized from hydrazine solution with (NH4)(2)Mo3S13 as the precursor at 180 degreesC for 16 h under hydrothermal conditions. The particles were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and high-resolution transmission electron microscopy (HREM). The influences of reaction conditions are C discussed while a mechanism is proposed to explain the formation of this peculiar morphology. (C) 2004 Elsevier Ltd. All rights reserved.
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