Journal
APPLIED SURFACE SCIENCE
Volume 268, Issue -, Pages 343-348Publisher
ELSEVIER
DOI: 10.1016/j.apsusc.2012.12.093
Keywords
Calcium phosphate; Electrodeposition; Electron microscopy; Corrosion; Biomaterial; Titanium alloy
Ask authors/readers for more resources
Calcium phosphate coatings are synthesized on titanium alloy (Ti6Al4V) substrates by pulsed electrode-position. This work aims to observe the morphological modifications of the coating when an amino acid is added to the electrolytic solution used in the process. The effects of two amino acids (glutamic acid and aspartic acid) are studied at a low and a high concentration. The coating morphology is observed at a nanometer scale by field emission gun-scanning electron microscopy (FEG-SEM). The structural characterization of the coating is performed by Fourier transformed infrared spectroscopy (FT-IR), Raman spectroscopy and X-ray diffraction (XRD). Moreover, corrosion measurements of the prosthetic surfaces are carried out by potentiodynamic polarization experiments in a physiological solution named Dulbecco's modified eagle medium (DMEM). The results show that the addition of an amino acid to the electrolytic solution leads to the decrease of the size of the crystallites which compose the prosthetic calcium phosphate coating that becomes denser and less porous than the coatings obtained without amino acid. Consequently, the corrosion behavior of the prosthetic material immersed in DMEM is improved. (C) 2012 Elsevier B.V. All rights reserved.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available