Journal
APPLIED SURFACE SCIENCE
Volume 257, Issue 21, Pages 8950-8954Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.apsusc.2011.05.070
Keywords
Graphene oxide; Zinc oxide; Nanorods; Hybrid
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Funding
- Shanghai Municipal Education Commission [09SG02]
- Shanghai Education Development Foundation
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This work presented a hybrid architecture of graphene oxide (GO)/ZnO nanorods (ZNs) with ZNs attached parallel onto GO sheets. ZNs were synthesized by refluxing zinc acetate dehydrate in methanol solution under basic conditions followed by surface modification of 3-aminopropyl triethoxysilane (ATS), and then the preformed ZNs were attached onto GO sheets by reaction of the amino groups on the outer wall of ZNs with the carboxyl groups on the GO surface. Transmission electron microscopy (TEM) image of the as-prepared hybrid reveals the morphology of the architecture of GO/ZNs hybrid. Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), thermogravimetric analysis (TGA) ultraviolet-visible (UV-vis) and fluorescence spectroscopy were also performed to characterize the structure and properties of the GO/ZNs hybrid. It was shown that ZNs maintained their initial morphology and crystallinity in the hybrid and the luminescence quenching of yellow-green emission of ZNs confirmed the electron transfer from excited ZnO to GO sheets. (C) 2011 Elsevier B.V. All rights reserved.
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