Journal
JOURNAL OF MATERIALS RESEARCH
Volume 19, Issue 8, Pages 2478-2486Publisher
CAMBRIDGE UNIV PRESS
DOI: 10.1557/JMR.2004.0316
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Using depth-sensing indentation, a pop-in phenomenon induced by grain boundaries, namely, a sudden indenter displacement jump when indented near a grain boundary segment, was observed in polycrystalline niobium. This grain-boundary type of pop-in occurs at a larger force than the initial elasto-plastic pop-in, which is observed with and without a grain boundary nearby. The experimental results show that this pop-in effect has a close relationship with the misorientation across the grain boundary. The occurrence of this pop-in phenomenon is rationalized in terms of slip transmission across the grain boundary.
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