Journal
SYNTHESIS-STUTTGART
Volume -, Issue 11, Pages 1806-1813Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2004-829126
Keywords
benzotriazole methodology; N-acylbenzotriazoles; acylating agent; S-acylation; thiol esters
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Diverse thiol esters were synthesized in good to excellent yields (76-99%) by reactions of thiophenol, benzyl mercaptan, ethyl mercaptoacetate, and mercaptoacetic acid with N-acylbenzotriazoles under mild conditions. These results demonstrate the utility of N-acylbenzotriazoles as mild S-acylating agents, especially when the corresponding acid chlorides are not readily available.
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