Journal
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES
Volume 807, Issue 2, Pages 217-221Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jchromb.2004.04.011
Keywords
rofecoxib
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A rapid and simple HPLC assay was developed for the determination of rofecoxib in human plasma and breast milk. After solid-phase extraction, rofecoxib was resolved on a C18 column and detected by UV detection at 272 nm. Standard curves were linear over the concentration range 10-2000 mug/L (r(2) > 0.99). Intra- and inter-day coefficients of variation for both matrices were <10% and the limit of quantification was around 10 mug/L. (C) 2004 Elsevier B.V. All rights reserved.
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