Journal
CATALYSIS LETTERS
Volume 97, Issue 3-4, Pages 155-162Publisher
SPRINGER
DOI: 10.1023/B:CATL.0000038578.67273.b0
Keywords
butyronitrile; INS; LiOH; Raney-Cobalt; surface modification; surface species
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Inelastic Neutron Scattering (INS) spectroscopy was used to characterize the catalytic hydrogenation of butyronitrile on the surface of parent and LiOH-modified Raney-Co. At low pressure hydrogen is mainly adsorbed on 3-fold sites. Co-adsorbed butyronitrile and hydrogen react on the unmodified Raney-Co sample to several partially hydrogenated products that contain N-H bonds. The nature of the species suggests that bi-molecular condensation leading to N-Butylidene-1-butanamine is feasible.
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