4.5 Article

Simultaneous DSC/FTIRS/TMA

Journal

MEASUREMENT SCIENCE AND TECHNOLOGY
Volume 15, Issue 9, Pages L5-L10

Publisher

IOP PUBLISHING LTD
DOI: 10.1088/0957-0233/15/9/L01

Keywords

polymers; Fourier transform near-infrared spectroscopy (FTIRS); differential scanning calorimetry (DSC); non-contact fibre optic thermal expansion; thermomechanical analysis (TMA)

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This paper reports, for the first time, on a novel technique which combines differential scanning calorimetry and Fourier transform near-infrared spectroscopy with a non-contact fibre optic thermal expansion probe to give simultaneous thermal, spectral and dilatometric information on a polymer sample. The experimental set-up is described in detail and the technique is demonstrated using a polypropylene film sample.

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