Journal
TETRAHEDRON LETTERS
Volume 45, Issue 41, Pages 7779-7781Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2004.08.054
Keywords
total synthesis; oxazinins; morpholinone; 3-methyleneindolenine
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A synthetic strategy, based on intramolecular addition of an appropriate hydroxyl substituent to a 3-methyleneindolenine, towards the naturally occurring marine toxins oxazinin-1, -2 and -3 is presented. The expedient first total synthesis of oxazinin-3, thus accomplished, demonstrated the efficiency of the approach and established the absolute stereochernistry of oxazinin-3 as 2S,5S. (C) 2004 Elsevier Ltd. All rights reserved.
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