Journal
ORGANIC LETTERS
Volume 6, Issue 21, Pages 3755-3758Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol048524h
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Alkoxycarbenium ions have been generated and accumulated as cation pools by the low-temperature electrochemical oxidation of alpha-phenylthioethers. Although an unsuccessful attempt to accumulate glycosyl cations was made, a one-pot method for electrochemical glycosylation, which involves anodic oxidation of thioglycosides to generate glycosyl cation equivalents followed by their reactions with glycosyl acceptors, has been developed.
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