Journal
ORGANIC LETTERS
Volume 6, Issue 21, Pages 3805-3808Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0484198
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(GRAPHICS) A reusable polymer-supported hydrophosphinylation catalyst is described for the preparation of H-phosphinic acids. The polystyrene-based ligand is prepared in one step from commercially available compounds. The polymeric catalyst generally gives good yields for a variety of substrates and is water- and air-tolerant, although the scope of alkenes and alkynes which can be employed is somewhat narrower than with our original xantphos/Pd(2)dba(3) Catalyst.
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