Journal
ORGANIC LETTERS
Volume 6, Issue 21, Pages 3655-3658Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol049160w
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A synthesis of a C4-epi-C1-C6 fragment of the antitumor agent FR901464 is reported. The advanced intermediate prepared in this study contains two of the three correct stereocenters found in the C1-C6 moiety of FR901464. For the preparation of this intermediate, we have developed a highly diastereoselective bromolactolization of a delta-alkenyl ketone.
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