Journal
ORGANIC LETTERS
Volume 6, Issue 22, Pages 3977-3980Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0483854
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[GRAPHICS] A general synthesis of acylsilanes from the corresponding morpholine amides and silyllithium species is described. The use of morpholine amides is economical and prevents over-addition by the silyl nucleophile. The procedure cleanly affords acylsilanes in good yields and circumvents the use of stoichiometric copper(I) cyanide typically employed to synthesize these compounds from acid chlorides.
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