Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 8, Issue 6, Pages 838-845Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op040006z
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The title compound was prepared from p-anisaldehyde and ethyl ethoxyacetate via a racemic synthetic route: The synthesis involves a Claisen-type condensation in which the elimination was unexpectedly promoted by an excess of the ester. The process has been successfully performed on a 2000-L scale with a total yield over seven steps of 19%.
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