Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 8, Issue 6, Pages 1059-1064Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op0498823
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A scale-up of a new process for the production of 2-chloro-5-trifluoromethyl-benzonitrile by a Sandmeyer reaction of 2-Chloro-5-trifluoromethylaniline with copper cyanide/sodium cyanide is described. To ensure a safe implementation, a safety evaluation of the process was carried out, which is described. in the following. The new process gives a better working environment and better productivity due to shorter reaction time.
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