Journal
CHEMISTRY OF MATERIALS
Volume 16, Issue 22, Pages 4324-4329Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm0494148
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The rock salt-type LiTiO2 and spinel-type LiTi2O4 were synthesized with accurate control of stoichiometry by electrochemical insertion of Li+ into solid TiO2 (anatase) in molten LiCl. The behavior of Li+ insertion was investigated by cyclic voltammetry using a TiO2 powder modified molybdenum electrode. The results indicate two Li+ insertion reactions at two different potentials for the formation of LiTiO2 and LiTi2O4, respectively, as confirmed by ICP, XRD, and TEM analyses.
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