Journal
MACROMOLECULAR CHEMISTRY AND PHYSICS
Volume 205, Issue 16, Pages 2229-2234Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/macp.200400204
Keywords
double crystalline diblock copolymer; PEO-b-PCL diblock copolymer; ring-banded spherulites
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The crystallization behavior of crystalline-crystalline diblock copolymer containing poly(ethylene oxide) (PEO) and poly(epsilon-caprolactone) (PCL), in which the weight fraction of PCL is 0.815, has been studied via differential scanning calorimeter (DSC), wide-angle X-ray diffraction (WAXD), and polarized optical microscopy (POM). DSC and WAXD indicated that both PEO and PCL blocks crystallize in the block copolymer. POM revealed a ring-banded spherulite morphology or the PEO-b-PCL diblock copolymer.
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