Journal
CHEMISTRY LETTERS
Volume 33, Issue 11, Pages 1430-1431Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2004.1430
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A photochemical [2+2] cycloaddition reaction was executed in a microflow system using glass-made microchannels having 1000-mum width and 500-mum depth. The reaction of cyclohexenones with vinyl acetates in a microflow system under irradiation (300 W, Hg lamp) gave [2+2] cycloaddition products in good yield with a residence time of 2h, which is a remarkably shortened reaction time compared with a batch system using the same light source.
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