Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 69, Issue 23, Pages 8121-8124Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo048713d
Keywords
-
Categories
Ask authors/readers for more resources
Stepwise amination of cyanuric chloride (1) with 5-(4-aminophenyl)-10,15,20-triphenylporphyrin (2) and/or its zinc(II) complex (3) enables the synthesis of porphyrin-porphyrin dyads with predetermined free base-free base forms or free base-zinc and zinc-zinc metalation states. Furthermore, the use of aminopropyl-silanized silica gel as a scavenger for unwanted byproducts allowed the one-pot synthesis of title porphyrin compounds in high yield and purity with minimum use of preparative column chromatography.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available