Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 70, Issue 1, Pages 391-393Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo048599z
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A mild protocol for the copper-free Sonogashira coupling of aryl iodides with terminal acetylenes in water under aerobic conditions has been developed. The use of 1 mol % PdCl2 in the presence of pyrrolidine allows the coupling reaction to proceed at room temperature or 50 degreesC with good to excellent yields.
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