Journal
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
Volume 381, Issue 3, Pages 656-659Publisher
SPRINGER HEIDELBERG
DOI: 10.1007/s00216-004-2939-9
Keywords
solid-phase nucroextraction; in-tube SPME; automation; gas chromatography
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An online device is described in which analytes are extracted from a liquid sample by means of in-tube solid-phase microextraction (in-tube SPME), pulse released by rapid heating, and transferred to a gas chromatograph in a fully automated way. Switching of the sample and gas flows as well as the heating of the extraction tube and the valves is controlled by a remote computer system. Results obtained for river water and for aqueous standard solutions of phenanthrene are presented and are compared to the performance of standard SPME.
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