Journal
TETRAHEDRON LETTERS
Volume 46, Issue 6, Pages 995-999Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2004.12.033
Keywords
isomeric cyclophanes; pyridinophanes; one-pot; four-centre; self-assembly
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A one-pot synthesis of structurally isomeric tetrathiacyclophanes through four-centre coupling reactions of suitable bromides and thiols is reported. The structures of the isomers were confirmed by spectroscopy and XRD analysis. Single crystal X-ray analysis reveals interestingly shaped molecular structures with large cavities. (C) 2004 Published by Elsevier Ltd.
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