Journal
BIOCONJUGATE CHEMISTRY
Volume 16, Issue 2, Pages 465-470Publisher
AMER CHEMICAL SOC
DOI: 10.1021/bc049752z
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Phthalimido-alkanol solid supports were rapidly prepared from solid supported phthalic anhydride and amino alcohol condensation induced by microwaves. These supports were used to synthesize 5'-fluorescent 3'-aminoalkyl oligodeoxynucleotides allowing a two-step deprotection necessary to avoid aminolink alkylation. After conversion into an NHS derivative using dissuccinimidyl suberate and an optimized isolation, they were conjugated with a protein.
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