3.8 Article

Survey of acrylamide in Turkish foods by an in-house validated LC-MS method

Journal

FOOD ADDITIVES AND CONTAMINANTS
Volume 22, Issue 3, Pages 204-209

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/02652030512331344178

Keywords

acrylamide; liquid chromatography; mass spectrometry method; in-house validation; survey of Turkish foods

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A survey of retail Turkish foods was conducted for acrylamide using an in-house validated LC-MS method. The recoveries obtained for a variety of food matrices ranged between 81.2 and 96.8% for a spiking level of 500 ng g(-1). The limit of quantification was determined as 15-20 ng g(-1) depending on the food matrix in the basis of a signal-to-noise ratio of 5. A total of 120 food samples were analysed for acrylamide. The mean acrylamide levels in different food groups were in the order: crackers > potato chips > biscuits > cakes > baby foods > corn chips > cookies > breakfast cereals > breads > grilled vegetables > wafers > chocolates. The crumb of bread was free of acrylamide, whilst significant concentrations were found in the crust.

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